Mike Patton & Jennifer Charles did a great job on Music to Make Love to Your Old Lady By by Lovage. Their voices complimented each other really well and a few of the songs actually sounded like they were having sex in some songs.
Another great male/female collab was Devin Townsend and Anneke van Giersbergen from The Gathering on Devin's album Addicted!. She didn't appear on every track, but she did appear on about half, one in which she did vocals and Devin played guitar.
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