If you want to hear the first psychedelic recording, it was made in 1962 and is called (rather aptly) "This Is It", and it's by Alan Watts.
...must check through the rest of the posts before suggesting anything else... although you MUST hear "Black Mass" by Jason Crest (1968), "Red The Sign Post" by Fifty Foot Hose (1968) and "Love Without Sound" by White Noise (Delia Derbyshire and David Vorhaus, 1969) - essential!!! :O)
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